Data File D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.DSample Name: BIZ2015-N06-WJ4=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 10Acq. Instrument : HY-LCMS-02 Location : P1-F-01Injection Date : 11/7/2015 1:46:23 PM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 10.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\100-1000MS+10MIN _1.5(0.02%FA)-BD.MLast changed : 11/7/2015 11:56:24 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\10-80A,18MIN(RP-HPLC).MLast changed : 11/10/2015 2:18:19 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B0803 Batch#18510 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.D) 6.200mAU250200150 7.701100 3.747 4.085 5.351 5.5945002 9.3578min46 ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 3.747 BB 0.0539 2.31854 6.78641e-1 0.0207 2 4.085 BB 0.1022 2.29890 2.97242e-1 0.0205 3 5.351 BV 0.0617 2.05274 5.02094e-1 0.0183 4 5.594 VB 0.1290 10.52177 1.19229 0.0941 5 6.200 MM 0.6808 1.10513e4 270.55881 98.7845 6 7.701 MM 0.0979 42.23842 7.18987 0.3776 7 9.357 MM 0.2517 76.54749 5.06920 0.6842 Totals : 1.11872e4 285.48814 ===================================================================== *** End of Report ***HY-LCMS-02 11/10/2015 2:18:22 PM Yang Qian(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.DSample Name: BIZ2015-N06-WJ4=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 10Acq. Instrument : HY-LCMS-02 Location : P1-F-01Injection Date : 11/7/2015 1:46:23 PM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 10.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\100-1000MS+10MIN _1.5(0.02%FA)-BD.MLast changed : 11/7/2015 11:56:24 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\10-80A,18MIN(RP-HPLC).MLast changed : 11/10/2015 2:21:07 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B0803 Batch#18510 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.D) ES-API, Pos, Scan 6.19770000060000050000040000030000020000010000002468min HY-LCMS-02 11/10/2015 2:21:09 PM Yang Qian(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.DSample Name: BIZ2015-N06-WJ4MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 6.197 31540892 533.20 I 532.20 I 531.20 I 530.20 I 529.20 I 528.20 I 528.2*MSD1 SPC, time=6.026:7.266 of D:\\AGLIENT 1260\\DATA\\20151107\\20151107 2015-11-07 11-56-24\\BIZ2015-N06-WJ4.D ES-API, Max: 1940917550250100200300400500600700800900m/z *** End of Report ***HY-LCMS-02 11/10/2015 2:21:09 PM Yang Qian(LCMS-02) 533.2Page 2 of 2